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Total synthesis, structural revision, and absolute configuration of (+)-clavosolide A
- Son, JB;
- Kim, SN;
- Kim, NY;
- Lee, DH
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50초록
Enantioselective synthesis of 3, a revised structure for clavosolide A, was completed. Both H-1 and C-13 NMR spectra of the natural and synthetic compounds were identical, and optical rotation measurements identified the absolute configuration of the natural clavosolide A as the enantiomer of 3.
키워드
1,5-ASYMMETRIC INDUCTION; SELECTIVE REDUCTIONS; ALKYL-HALIDES; ASSIGNMENT; GLYCOSIDES; FRAGMENT; HYDRIDE
- 제목
- Total synthesis, structural revision, and absolute configuration of (+)-clavosolide A
- 저자
- Son, JB; Kim, SN; Kim, NY; Lee, DH
- 발행일
- 2006-02-16
- 유형
- Article
- 저널명
- Organic Letters
- 권
- 8
- 호
- 4
- 페이지
- 661 ~ 664
- 언어
- ENG
- 출판사
- American Chemical Society
- 발행국가
- 미국
- 분량
- 4 페이지
- ISSN
- E 1523-7052
P 1523-7060